- Method Development
- Method Validation
- Method Transfer
- Sample Testing
METHOD DEVELOPMENT
Our extensive knowledge and analytical tools can help you achieve precise and accurate testing conditions for the analysis of samples.
Our crew of scientists will be happy to facilitate you with various compound method development. Our team is experienced and qualified in analytical techniques and instrumentation such as HPLC, GC, LC, and MS/MS. We research initially to determine the following:
- Compound solubility.
- Chemical and physical properties
- Instrumentation.
- Sample preparation.
- Concentration range
- Limit of detection and Limit of Quantification.
We provide on-site and off-site consultation for your new product and compound method development.
METHOD VALIDATION
Method validation plays a key role to determine whether the test method used for analysis has optimum work and analytical conditions. We have experts who can facilitate you in deciding the validation parameters for your compound of interest.
Our team is qualified to perform simple to complex method validation with accurate results. Our validation process includes Initial consultation, determining parameters (Accuracy, precision, robustness, Intermediate precision, Validation protocol, performing and documenting Validation and creating a summary report, updating clients promptly. We follow the below guidelines for validation and update additional experiments whenever needed.
- ICH Harmonized Tripartite Guideline Validation of Analytical Procedures: Text and Methodology Q2(R1) November
- World Health Organization (WHO), Guidelines on Validation – Appendix 4 Analytical Method Validation, September 2018
- USP-NF <1224> Transfer of Analytical Procedures
- USP-NF <1225> Validation of Compendial Procedures
- USP-NF <1226> Verification of Compendial Procedures
METHOD TRANSFER
Synergy perform Method Transfer of existing methods from other laboratories and Method verification for Compendial methods.
SAMPLE TESTING
We have preferred partners to perform analytical testing of various tests such as:
Wet chemistry (LOD, Dissolution, ID by IR, TOC, and so on.),
Assay testing,
impurity testing,
and trace analysis (Quantitative and Qualitative)
using respective instrumentation (LC, ICP, GC, GCMS, LCMS) techniques. We are experts in handling different categories such as natural health products or dietary supplements, raw materials, and finished products. We offer on-site consultation for various cannabis test methods and matrices. Spectra of our proficiency in complex matrix analysis will help to reach enormous goals.